The Viking missions to Mars

Pyrolitic release experiment

"Of the three Viking biology experiments, only the PR experiment approximated actual martian surface conditions and did not use water. In this experiment, a 0.25-cc soil sample was incubated in a simulated martian atmosphere of CO2 and CO labeled with carbon-14. A xenon arc lamp provided simulated sunlight. After 5 days, the atmosphere was flushed and the sample heated to 625 degrees C (1157F) to break down, or pyrolyze , any organic material, and the resulting gases were passed through a carbon-14 detector to see if any organisms had ingested the labeled atmosphere."

http://cmex-www.arc.nasa.gov/MarsEssy/life/life.htm

Result: Carbon detected.

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